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Informational Letters

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Informational Letter IL 99-2

28 May 1999

TO: All Oil and Oil Sands Operators

USE OF PRODUCED SAND IN ROAD CONSTRUCTION

EXECUTIVE SUMMARY

Significant volumes of reservoir (produced) sands are produced along with heavy oil in northeast Alberta. The EUB classifies this produced sand as "non-dangerous oilfield waste."

The heavy oil industry has been actively investigating a range of options for the safe re-use and/or disposal of this sand. Recently, using this sand in roadbed construction has become a significant disposal option.

A task force was formed to determine guidelines for produced sand use in roadbed construction. Participation of various stakeholders included environmental groups, the public, the heavy oil industry, waste processors, Alberta Transportation and Utilities, Alberta Environmental Protection, and the EUB. The attached IL is the result of extensive research and review by the task force. The recommendation that this practice be allowed is based on extensive and rigorous scientific research and opinion.

The EUB is prepared, under very restricted conditions (strict limits on contaminants for example), to allow this sand to be incorporated or encapsulated into roads during construction. The primary contaminants of concern are chlorides (salt) and hydrocarbon (oil). As such, two key restrictions are:

  • the chloride concentration of sand encapsulated into roads must not exceed 3000 milligrams per kilogram, and
  • the concentration of entrained crude oil in the sand cannot exceed five per cent.

Other conditions will also apply, including strict controls limiting contaminants such as free water, benzene, or heavy metals. In addition, the produced sand must not be contaminated by any sources of halogenated hydrocarbons, hazardous chemicals, refined or lube oils, drilling waste, flare pit sludge, or spill clean-up materials or any other deleterious materials. Requirements for storage and sampling of the produced sand are also set out.

Companies must follow a clearly defined application process that involves both the EUB and the local county or municipal district. The appropriate EUB Field Centre will issue an approval to use produced sand in road construction, should a tendered application meet all EUB requirements.

The EUB notes that, because of varying native soil properties and other geographical features, not all roads are suitable for using produced sand during construction. The Board expects the local county or municipal district accepting the produced sand and the oil company which generated the material to carefully evaluate site characteristics and ensure proper practices are adhered to.

Failure by a company to comply with the requirements of the new guidelines will result in EUB enforcement actions, which may include immediate suspension of the road project and immediate implementation of corrective action. Future approvals for using produced sand in road construction may also be withheld.

A key issue considered in formulating this guideline was who would be liable for any environmental contamination that might result from using produced sand in roadbed construction? Both the task force and Board sought legal advice on this question.

The understanding of the Board, based on that advice, is that there are four parties that could potentially be held liable for addressing any contamination. These parties are: owners and past owners of the produced sands, those in charge, management and control of the produced sands, directors and officers of the companies and successor companies that generated the produced sands, and owners and past owners of the roads.

These guidelines will be subject to review every two years, or as necessary.


1 INTRODUCTION

This Informational Letter outlines the EUB guideline for produced sand to be used as construction material in roads. The produced sands referred to in this document are limited to the solids (reservoir sand) recovered from heavy oil operations in north-east Alberta. This material contains small quantities of hydrocarbons and chlorides and may be used in road construction in accordance with this document.

This guideline, includes criteria, site restrictions, application requirements, audit, and enforcement expectations for produced sand generators.

As a companion to Part F Section 29.0 "Spreading of Oily By-Products to Roads" in Guide 58, Oilfield Waste Management Requirements for the Upstream Petroleum Industry, this guideline will be subject to regular review every two years or as required. Further, it will be added into Guide 58 in due course. Some of the terminology used in this guideline have been given specific definitions, as noted below, which are consistent with road construction practice but may not necessarily match other accepted definitions for those terms.

Produced Sand

Reservoir sand (oily by-product material) with small quantities of hydrocarbon and chloride typically stung (the practice of using a washing wand and vacuum truck to recover the sand) or augured from production tanks in heavy oil operations.

Incorporation

Mixing of the produced sand and native clay to a uniform consistency during road construction.

Encapsulation

Encasement of produced sand into an impervious roadbed cell.

Statutory Road

Designated municipal road or highway


2 CHARACTERISTICS OF PRODUCED SAND

Based on the characteristics noted below, produced sand is typically classified as non-dangerous oilfield waste and therefore, is equivalent to waste classified as non-hazardous under the Alberta Environmental Protection and Enhancement Act, Waste Control Regulation. Produced sand typically found in north-east Alberta, generally falls within the ranges for the parameters1 listed here:

flashpoint

greater than 61 degrees Celsius

total petroleum hydrocarbon

10 000 to 150 000 mg/kg (using Dean Stark Method)

chloride

200 to 30 000 mg/kg

sodium

150 to 20 000 mg/kg

trace metals

similar to soil background values

particle size

fine to very fine sand (250 to 62.5 microns)

pH

6 - 8

1 Established from EUB and industry databases. Variances are the result of different reservoir conditions and operator production and storage practices.

Although the information indicates that within produced sand the concentrations of crude oil, sodium, and chloride can range drastically, the average concentrations typically found are around 3.5 per cent or 35 000 mg/kg oil, 2000 mg/kg sodium, and 3500 mg/kg chloride. Considering that 93 per cent or more of the components within heavy crude oil boil at a temperature greater than 225 C, the residual crude oil within the produced sand is of high molecular weight and therefore, monoaromatic hydrocarbons (benzene, toluene, ethylbenzene, and xylenes) occur at extremely low levels.

Although the pH of produced sand typically ranges from 6 to 8, the receiving road material would easily buffer a pH range between 4 and 9. Therefore, the requirement to measure the pH of the produced sand has been dropped from the criteria listed below.

Publications and scientific literature relating to road construction practices indicate that higher molecular weight hydrocarbons such as bitumens and asphaltenes are used as soil stabilizers in the preparation of road sub-bases and grades. The literature also indicates that the presence of sodium in clay material decreases the permeability of the admixed soils while chlorides provide additional stabilization and freezing point depression. Relating this information to the characteristics of produced sand, the Task Force deems that produced sand is an acceptable construction material for roads and poses minimal environmental and safety risks provided the criteria and requirements set out below are met.


3 CRITERIA

Produced sand generated during in situ oil sands and heavy oil production in north-eastern Alberta may be incorporated or encapsulated into roads during their construction provided the following criteria are met:

3.1

The chloride concentration in the produced sand must not exceed 3000 mg/kg. The 1:9 water extraction method shall be used to analyze the concentration of chloride in the produced sand.

Note:

Taking into consideration a road functions as a commercial/industrial use and not as an agricultural field, the chloride limit was calculated by relating it back to the CCME commercial/industrial value for EC, which is 4 dS/m.

3.2

The concentration of crude oil entrained in the produced sand does not exceed 5 per cent as determined using the Dean Stark toluene soxhlet extraction method. Information must be available that verifies the crude oil from which the produced sands are recovered has a density greater than or equal to 920 kg/m3.

3.3

The produced sand must have a flashpoint greater than 61 C.

Note:

Operators of sand storage facilities may eliminate the necessity to analyze the produced sand for flashpoint provided they have sufficient information to demonstrate the flashpoint meets the criteria, the source of sand has not changed, and the production process has not changed.

3.4

The produced sand shall be incorporated at a rate of 1 part sand to 3 or more parts native road construction material or encapsulated such that the volume of sand within the encapsulated lens does not exceed 25 per cent of the entire road construction material.

3.5

Every reasonable effort shall be made to minimize free water within the produced sand storage facility. Prior to disposition free water on the surface or lying within the storage facilities must be removed.

3.6

The produced sand must not be contaminated by any sources of halogenated hydrocarbons, hazardous chemicals, refined or lube oils, drilling waste, flare pit sludge, or spill clean-up materials or any other deleterious materials.

3.7

The produced sand must be analyzed for strong acid digest metals using US EPA method 3050 or 3051 and compared to the following CCME (Agricultural) criteria:

Cd
Hg
Pb
Ni
Cu
Zn

1.4
6.6
70
150
63
200

Note:

Except for nickel, the above metal concentrations have been taken from the 1997 CCME Recommended Soil Quality Guidelines for agricultural soils. The nickel concentrations are from the CCME 1991 criteria for agricultural soils. As the concentrations of metals within produced sand are typically similar to soil background values, levels exceeding the above concentrations could be an indication that other wastes/materials have been mixed with the produced sand. Operators may eliminate the necessity to analyze for metals provided they have sufficient information that concludes the metals don't exceed the above criteria, the source of the sand has not changed, and the production process has not changed.

3.8

The produced sand must be analyzed for total BTEX using EPA method 8240 or 8020 and shall not exceed the following criteria taken from the 1997 CCME Recommended Soil Quality Guidelines for residential/parkland soils.

benzene
ethylbenzene
toluene
xylene

0.5 mg/kg
1.2 mg/kg
0.8 mg/kg
1.0 mg/kg

Note:

Although a road functions as a commercial/industrial use, the Task Force acknowledges that in a rural setting a road would be adjacent to residential, parkland, or agricultural land. Considering the concerns related to BTEX components, it was deemed that it would be prudent to not potentially expose adjacent land uses to industrial levels for BTEX. Furthermore, as the volume of produced sand used in road construction cannot exceed 25 per cent of the entire road material, it was deemed that parkland/residential levels would protect adjacent land uses, including agricultural. Operators may eliminate the necessity to analyze for BTEX provided they have sufficient information that concludes the BTEX components do not exceed the above criteria, the source of the sand has not changed and the production process has not changed.


4 STORAGE FACILITY MANAGEMENT

4.1

Operators under the jurisdiction of the EUB must store all materials used, produced, and generated on their sites in accordance with EUB ID 95-3 and Guide 55, Storage Requirements for the Upstream Petroleum Industry. In addition to storing the produced sand in a facility that complies with the storage requirements, produced sand from tank bottoms must be stockpiled separately from other materials that may be placed in the same storage cell (e.g., spill materials). It is the responsibility of the operator to ensure that:

  • produced sand is segregated from other materials,

  • the sand stockpile is accessible for sampling,

  • water within produced sand storage facilities be managed by controlling or removing any free water, and

  • the sand is kept separate from other material once it has been sampled (i.e., no extra sand being added to the sampled pile).

5 SAMPLING PROCEDURES

5.1

Operators of sand storage facilities are responsible to ensure representative samples are obtained from sand stockpiles that are to be used in road construction. Appropriate sampling methods, such as those in Appendix 1 "Recommended Practices of Sampling Protocol for Roadbed Construction", must be used to obtain a representative composite sample. If the sand stockpile is over 2.5 metres (m) in height, the following also applies:

  • sampling is required for each 1.5 - 2.5 m intervals,

  • as each interval is sampled, it must be removed and stacked, or segregated from any additional materials entering the storage facility, and

  • no additional material can be added to the pile after the samples have been taken.
5.2

The representative composite sample for every 1.5 - 2.5 m of sand within the sand storage facility must be analyzed for parameters outlined in Section 3 of this document. The results of the analyses must be recorded on the Produced Sand Characterization for Roadbed Incorporation/Encapsulation Data Sheet, which is found in Appendix 2, and then submitted to the recipient (local authority) and the appropriate EUB Field Center office.

5.3

For audit purposes and for comparison to the storage facility analyses, samples shall be taken of the produced sand during road construction activities by the operator and handled in the following manner:

  • for each kilometre (km) of road, eight - one litre samples shall be taken as the trucks are unloading to make a representative composite sample; less may be used if the length of the road is reduced, and

  • the composite samples must be retained (stored in 1 litre (L) glass jars sealed tightly with a teflon lid at a temperature of 4C) for a period of one calendar year, and

  • as the result of the road construction project being audited or at the request of the EUB, these samples must be analyzed for the characterization parameters identified in Section 2, including BTEX, and compared to the criteria limits identified in Section 3 and to the analyses from the sand storage facility. These results must also be submitted to the local authority (MD/County) and appropriate EUB Field Center office.

Note: At the request of the EUB, additional sampling and analyses may be required.


6 SITE CHARACTERISTICS AND RESTRICTIONS

As a result of native soil properties and other geographical features, not all roads will be suitable for the encapsulation or incorporation of produced sand during their construction. In addition to the produced sand meeting the criteria specified in Section 3.0, the following road site characteristics and restrictions provide added environmental protection against the potential migration of salt or hydrocarbon contained within the produced sand used in a road construction project.

It is the responsibility of the local authority (county/municipal district) and operator (generator of the produced sand) to ensure these site characteristics and restrictions are adhered to. It is also expected that roads having produced sand incorporated or encapsulated into them, must be constructed following acceptable engineering practices (current Alberta Transportation and Utilities Standard Specifications for Highway Construction). The local authority, by allowing produced sand to be used as a road construction material, must agree that it will be used in accordance with this document.

6.1

The native soil of the selected road site shall:

  • have an electrical conductivity that does not exceed 2 dS/m (determined on a saturated paste extract) to ensure excessive salt loading is prevented, and

  • be clayey, meet the criteria for durable roads (minimum plasticity index of 15 per cent, minimum liquid limit of 30 per cent, and minimum clay fraction of 20 per cent), and occur to a minimum depth of 1.6 m (five feet) below the base of the produced sand.
6.2

The suitability of the existing soil type of the selected road must be assessed on site and confirmed by lab analyses.

  • test holes must be drilled every 200 m to a depth of 1.6 m. If the soil type changes based on field testing for electrical conductivity and clay content, the point in the road where the change occurs must be determined. Produced sand cannot be added past that point.

  • provided that the soil type does not change noticeably, analysis of one soil sample every 1.6 km by a certified lab is required to confirm suitability of the soil (electrical conductivity, plasticity index, liquid limit, per cent clay). Material representing the entire profile to 1.6 m depth must be submitted as part of the soil sample.
6.3

The following restrictions apply to roads selected for construction with incorporated or encapsulated produced sand:

  • only statutory road allowances shall be used. This is to ensure road allowances cannot be cancelled or abandoned,

  • the road shall be a minimum of 30 m horizontally from the high water mark of any surface body of water; roads that are likely to contact a surface body of water cannot be used,

  • the road shall not be within 100 m of a private or community water well or dugout, and

  • the produced sand must not be incorporated or encapsulated within 30 m of any culvert installed through the road.

Note: Future pipeline crossings must be bored under these roads. The bore hole must be a minimum of 1.2 m below the incorporated or encapsulated sand. An alternative procedure that will not compromise the integrity of the produced sand within the road may be acceptable.

6.4

For roads constructed with produced sand incorporated into them, the incorporation thickness (mixture of produced sand and native road material) shall not exceed 2 m. In addition, the produced sand shall be spread and uniformly mixed with the native road material at a ratio of 1 part sand to 3 or more parts road material to produce a homogeneous mixture, such that the electrical conductivity will not exceed CCME commercial/industrial criteria (Section 3.1).

Note: The produced sand must be delivered, spread, and incorporated into the road all within the same day. Produced sand must not be allowed to migrate off the road during or after construction.

6.5

For roads constructed with produced sand encapsulated into them, the produced sand cell shall not exceed a depth of 0.45 m and be limited to a single layer within a road. The volume of sand within the encapsulated cell shall not exceed 25 per cent of the road material. In addition, the clayey roadbed material encapsulating the produced sand cell (above, below and on the sides) shall be a minimum compacted thickness of 0.6 m. Each produced sand cell must be horizontally separated with a minimum of 2 m of compacted clayey roadbed material.

Note: Produced sand having a high silt content (greater than 30 per cent), based on particle size distribution, must not be encapsulated due to frost heave problems. The size of the produced sand cell is defined as the amount of produced sand that can be delivered, spread, and encapsulated within one day. The produced sand within a cell cannot be left exposed on the road overnight or during periods of precipitation. Produced sand must not be allowed to migrate off the road during or after construction.

6.6

The operator is responsible to ensure the engineering plans and as-built plans for the road construction project incorporating or encapsulating produced sand, as identified in Appendix 6, are prepared and completed. The local authority is accountable for the road and thus responsible to ensure road construction projects incorporating or encapsulating produced sand comply with the site characteristics and restrictions identified in this section. The engineering plans and as-built plans must be retained by the local authority in perpetuity, so that appropriate precautions will be taken if a road that has produced sand incorporated or encapsulated in it, requires future work.


7 APPLICATION PROCESS

7.1

If the produced sand is acceptable for road construction (incorporation or encapsulation), the operator must, prior to the commencement of the incorporation/encapsulation activities, provide the following information to the recipient (local authority) and the appropriate EUB Field Center office for review:

  • a copy of the Produced Sand Characterization for Roadbed Incorporation/Encapsulation Data Sheet (Appendix 2). The data sheet must be signed by a representative from the laboratory and by the operator. The data sheet must confirm that the sand is non-dangerous oilfield waste (non-DOW), and

  • a copy of the Application/Approval for Roadbed Incorporation/encapsulation Check Sheet (Appendix 3), and

  • a map outlining the section of road to be used for incorporation or encapsulation, the legal land description of that road, and confirmation that the Engineering Assessment has been done, and commitment that the site characteristics and restrictions in Section 6.0 will be adhered to.
7.2

The operator shall have written consent that the recipient (local authority) agrees to have produced sand incorporated/encapsulated into the road and that it will only be used in accordance with this document . A copy of the written agreement shall be submitted to the appropriate EUB Field Center office with the information from 7.1 above. Directly adjacent landowners/residents to the proposed road shall be notified of the project. A letter or documented personal visit from the recipient of the produced sand at least one week before construction begins would be considered appropriate notice. Operators must include information regarding any complaints following the landowner/resident notification.

7.3

Operators must discuss any potential applications, which may deviate from the requirements of this document for any reason, with the appropriate EUB Field Centre Office.


8 APPROVAL

8.1

Approval by the appropriate EUB Field Centre Office shall be granted if the above information is received and meets all EUB requirements and the operator ensures the items below are met. The operator shall then proceed with the method of incorporation encapsulation, to the indicated road, at the appropriate depth/mix. Any concerns or appeals regarding an approval must be made to the appropriate EUB Field Centre.

8.2

The operator and the receiver (local authority), shall ensure the following requirements are met during incorporation/encapsulation activities:

  • the produced sand is used in road construction according to good engineering practices, and Section 6.0 Site Characteristics and Restrictions are adhered to,

  • no product is lost during transportation of this material from the storage area to the incorporation/encapsulation point (e.g., by using truck tarps, if necessary), and

  • the appropriate EUB Field Center office shall be notified once incorporation/encapsulation operations have commenced.

The approval may be rescinded at any time should the produced sand not meet criteria or the operator fails to meet the requirements set out above.


9 SUPERVISION

9.1

The generator of the produced sand (operator) is responsible to complete an On-site Incorporation/Encapsulation Check Sheet(s) (Appendix 4), or the equivalent. The receiver will complete similar information. This is needed to ensure the following items are addressed and that the incorporation/encapsulation is being carried out as per the approval:

  • the produced sand being hauled to the road construction site is from the pile that was analyzed,

  • the transportation of the produced sand is being carried out in a satisfactory manner,

  • the produced sand is being applied as per approval (i.e., proper mix ratio and location),

  • grab samples are taken as the trucks are unloading and then used to make up a composite sample as outlined in Section 5.3. Information must be recorded on the Daily Road Information Check Sheet (Appendix 5), and

  • all details of this document and approval are being followed.
9.2

The operator must ensure that each road construction project is adequately managed by monitoring the project and ensuring the check sheets are completed for each project and submitted to their project file and retained for a minimum of two years.


10 COMPLIANCE AND ENFORCEMENT

10.1

Failure to comply with the requirements outlined in this document shall result with the EUB taking the following actions:

  • Immediate suspension of the road project,

  • corrective action to remedy the situation shall be performed immediately, and/or

  • withhold future approvals for road incorporation/encapsulation.
10.2

The EUB will determine the significance of the event (minor, major, serious) as defined below, in accordance with the EUB Generic or Field Surveillance Enforcement Ladders.

  • Minor Non-compliance Issue defined as a contravention of regulation(s)/requirement(s) which does not result in a direct threat to the public and/or the environment and does not adversely effect oil and gas operations. An example is missing information on a data sheet.

  • Major Non-compliance Issue defined as a contravention of regulation(s)/requirement(s) that an operator has failed to address and/or has the potential to cause an adverse impact on the public and/or the environment. An example is the quality of produced sand, as determined by the original analysis is significantly different from control sample analysis taken while produced sand is being incorporated or encapsulated. Another might be where a produced sand cell is left exposed overnight.

  • Serious Non-compliance Issue defined as a total disregard for regulation(s)/requirement(s) that is causing or may cause a significant impact on the public and/or the environment. An example is encapsulation or incorporation of produced sand without approval to do so.

Enforcement consequences for any non-compliance issues will be taken to ensure regulatory requirements are being met and operators are treated in a similar fashion. The enforcement actions taken by the EUB will be determined based on the severity of non-compliance, in accordance with the EUB Generic and Field Surveillance Group's enforcement ladders.

Actual definitions of minor, major, and serious non-compliance issues and examples of consequences relating to this document will be developed as part of the audit process (expected completion 15 June 1999). A copy can be obtained by contacting the appropriate EUB Field Center.

10.3

The appropriate EUB Field Center will conduct audits on a minimum of 10 per cent of the incorporation/encapsulation operations. The emphasis of the audits will be on compliance with the quality criteria specified for the produced sand and on accountability of the operator by ensuring the check sheets have been properly completed and signed. Corrective action resulting from the audit will be consistent with the consequences noted in 10.1 and 10.2 above.


11 PRODUCED SAND (WASTE) TRACKING

Section 9.0 of EUB Guide 58, Oilfield Waste Management Requirements for the Upstream Petroleum Industry, requires oilfield waste generators to implement and maintain a waste tracking system for the oilfield wastes listed on Table 9.1, Reportable Oilfield Wastes. As produced sand is an oilfield waste that is listed on Table 9.1, it must be tracked from the point of initial generation to final disposition. A road that has been constructed with produced sand incorporated or encapsulated into it, would be considered a final disposition point for the produced sand. Therefore, the volumes of produced sand used in the road construction and the location of the road must be recorded in the tracking system.

All tracking systems must be effective and capable of displaying due diligence. At any time, the EUB may audit a generator's waste tracking system or request the generator to provide information pertinent to the waste tracking system. As well, generators must be able to summarize the tracking information into an oilfield waste disposition report. For further information on oilfield waste tracking and reporting please refer to Part C, Guide 58.


12 LIABILITY

Although the Task Force believes produced sand is an acceptable construction material for roads and poses minimal environmental and safety risks, a key issue considered was who would be liable for any environmental contamination that might result from the use of produced sands in road construction. While the final answer to such a question may ultimately reside with the Courts, the Task Force and the Board did obtain legal advice on the question. The understanding of the Board, based on the results of that review, is there are four general parties that could potentially be held liable for addressing any contamination that might occur. These are:

  • owners and past owners of the produced sands,

  • those in charge, management, and control of the produced sands,

  • directors and officers of the companies and successor companies that generated the produced sands, and

  • owners and past owners of the roads.

On the basis of the above, the Board believes that landowners whose property abuts onto roads incorporating/encapsulating produced sand should not, provided that they do not also fall into one of the above categories, face any liability or bear any subsequent responsibility for clean up to either their land or water, in the unlikely event that contamination might arise from the use of produced sand as road construction material.

[Original signed by]

J. D. Dilay, P.Eng.
Board Member


Attachments

APPENDIX 1: Recommended Practices of Sampling Protocol for Roadbed Construction

1 SAMPLE COLLECTION

1.1 Core Sampling Method

A representative sample must be obtained from each sand storage facility whose contents are to be used in the incorporation/encapsulation project in questions. The preferred method is to collect a composite sample made up of sub-samples collected from a grid pattern spaced evenly across the storage facility. The full depth of the produced sand is to be sampled if possible, or every 1.5 – 2.5 m interval.

As a rough guide to sampling intensity for pits less than 500 square m in area, a inimum of 5 sub-samples should be taken. For pits greater than 500 square m in area, a minimum of 9 sub-samples should be taken. The sub-samples should be mixed together into 1 composite sample.

Sub-samples should be collected using Shelby Tubes or hollow metal or PVC tubes 50 - 75 mm in diameter and sufficient length, or with sufficient extensions, to sample the full depth of the produced sand.

Prior to sampling a sand storage facility, the core sampler should be thoroughly cleaned to avoid cross contamination of the samples. This can be done using a steam cleaner or a three-stage process like the following example: The first stage cleaning should be done with an oil solvent, such as varsol and a wire brush and clean rag pull-through. The second stage should be done by rinsing with acetone or hexanol, until a clean cloth can be pulled through. Finally, a distilled water rinse should be used to remove any residue from the sampler.

NOTE: For produced sand stockpiles of a height greater than 2.5 m, sampling is required every 1.5 – 2.5 m interval.

1.2 Backhoe Method

An alternate method for taking the samples is to collect representative samples using a backhoe. Sub samples should be collected using a grid pattern similar to that described for core sampling. The full depth of the produced sand should be included in the subsample as much as possible.

It is not practical to wash the backhoe bucket in a similar fashion to that described for core sampling. Therefore, in order to ensure that the sub-samples do not become contaminated by mixing with previously sampled materials, enough of the material contained in each bucket must be sliced away using a clean spade or trowel so that a subsample slice or representative grab sample can be taken away from the sides of the bucket. Prior to sampling the pit, or tank, the sampling tool must be cleaned using the three stage wash similar to the one described for core sampling.

2 SAMPLE HANDLING

Sub-samples from the field containers (usually 20 L high density polyethylene pail) should be taken following the protocol below:

  • visually examine the sample,

  • combine sub-samples in a field container and mix thoroughly to form a composite sample,

  • take sample from field container and place in a clean (1 L) glass jar with a Teflon-lined lid.

The sample jar must be immediately labelled with a unique identification number and the sample identification sheet must be filled in. The jar must be properly labelled to comply with WHMIS requirements.

A copy of the sample sheet, including the Produced Sand Characterization for Road Incorporation/Encapsulation Data Sheet, must be sent with the sample to the laboratory.

Due to the complexity and precision in this analytical program, operators are requested to use a major laboratory qualified to analyze produced sand samples specific to the needs of produced sand characterization.

Note: The above sample collection and handling methodologies were developed jointly by industry, government and chemical laboratories using accepted industry standards modified for unique heavy oil operations. Any proposed alternate sampling method must provide a level of protection which, in the EUB's opinion, is equal to or greater than these requirements and must receive EUB approval

APPENDIX 2: Produced Sand Characterization For Road Incorporation/Encapsulation Data Sheet

 Appendix 2

Produced Sand Characterization For Road Incorporation / Encapsulation Data Sheet

Laboratory Name: ___________________ Lab Sample Number: _______________
Date Received:_______________ Field Sample Number: _________________ Date Analyzed: _____________

Sample Information

Operator:

Source: (i.e. ecology pit, desand tank etc.)

Pit Location : LSD __ __ __ __W M

Proposed Volume:

Pit Name_________________________________

Road Location: from LSD __ __ __ __W M to LSD __ __ __ __W M

Total Petroleum Hydrocarbons (Dean Stark Soxhlet Extraction Method)

1:9 Water Extraction Method

Particle Size Distribution

Soil Sampling Methods of Analysis
Hydrometer or pipette method – (Carter)

(Encapsulation Only)

Oil Concentration: (< 5 %)

%

Chloride/Cl: (<3,000mg/kg)

mg/kg

Total Metals (US EPA 3050 or 3051 (SW 846))

.

Concentration

.

Concentration

.

Concentration

% Silt (< 30 %)

Cadmium/Cd (<1.4)

mg/kg

Nickel/Ni (<150)

mg/kg

Lead/Pb (<70)

mg/kg

% Clay

Mercury/Hg (<6.6)

mg/kg

Zinc/Zn (<200)

mg/kg

Copper/Cu (<63)

mg/kg

% Sand

Total BTEX (EPA Method 8240 or 8020)

Flashpoint (Pensky- Martens Closed Tester ASTM D93-80)

.

Concentration

.

Concentration

(>61OC)

°C

Benzene (<0.5 mg/kg)

mg/kg

Toluene (<0.8 mg/kg)

mg/kg

Ethylbenzene (<1.2 mg/kg)

mg/kg

Xylene (<1.0 mg/kg)

mg/kg

.

The undersigned hereby certifies that the information is accurate and in accordance with the requirements of Section 3.

Signed: ___________________ (Laboratory Representative) _____________________ (Operator Representative)

  1. Produced sand sample must not contain halogenated hydrocarbons, hazardous chemicals, refined or lube oil, flare pit sludge, or deleterious substances such as filters, rags, vegetation, and other debris including significant volumes of contaminated agricultural soils.
  2. Information must be available that verifies the crude oil from which the produced sands are recovered has a density greater than 920 kg/m3.

 

APPENDIX 3: Application / Approval for Road Incorporation/Encapsulation

Please indicate with an (x) which type of submission

EUB File #

Initial Application or

EUB Signature :

Final Submission (incorporation/encapsulation completed)

EUB Approval Date :

General Information
Operator Name: _____________________________________________ _________
Local Authority (County/MD): ___________________________________________________
Engineering firm responsible for design of road: _____________________________________
Contractor building the road: ____________________________________________________
Is written consent from Local Authority (MD/County) as per Section 6.0 and 7.2 attached? (Yes/No) ________

Sand Information
Storage Facility location: LSD:_____________________ Pit Number/Name:______________________
Produced sand only: (Yes/No) ________ Proposed volume for this road: ________ m;
Proposed dates of incorporation/encapsulation: From: __________________To: _________________

Sand Sampling/Analysis Information
How was sampling done? (Core/Backhoe method) _________________ Sampling depth: _________m
Date of analysis: _____________ Are initial analysis attached? (Yes/No) _______
Oil content: ________ % by volume Chloride Concentration: ______ mg/k Silt _____ % (For encapsulation only)
Are more analyses required? (1 sample every 1.5 – 2.5 metres depth of stockpile) (Yes/No) _______
If yes date sampled: Date of analysis:
Are additional analyses attached: (Yes/No) _______

Consultation Information
Have all directly adjacent landowner/residents been notified? (Yes/No) ________

Road Information
Road location: From: LSD: _________________W__M To: LSD:__________________W__M
Has Engineering assessment been done? (Yes/No)______ Background Soils Properties: EC _____dS/m
Plasticity Index: ______% Liquid limit: _____% Clay Fraction _____% Are initial analyses attached? (Yes/No)________

Final Submission:
Was cell/trucks unloading sample analysed? (Yes/No) _______
Is cell/trucks unloading information attached? (Yes/No) ______ Actual amount of sand incorporated: _______ m3

Produced Sand Owner/Representative

Name: ____________________ Signature:____________________ Date:_______________

(print name)

NOTE:

By signing this form as a representative of the operator, I agree to follow the requirements for the use of produced sand in road construction, including adherence to Section 6.0 Road Site Characteristics and Restrictions.

APPLICATION:

For EUB approval, a copy of this sheet and the following must be submitted: written consent from MD/County, a copy of the initial analyses, and notification list.

FINAL SUBMISSION:

Please submit this sheet to Local Authority and EUB with all supporting documents, extra analyses, etc.

APPENDIX 4: On-Site Incorporation/Encapsulation Check Sheet

APPENDIX 4

* Submit to MD or County and retain on file EUB File Number: ____________

ON-SITE INCORPORATION/ENCAPSULATION CHECK SHEET

Yes

No

Remarks

Please submit this sheet to Local Authority and EUB with all supporting documents, extra analyses, etc.

. . .

Do you have a copy of the EUB Approval?

. . .

Is resample required due to depth of stockpile?

. . .

Is the produced sand segregated from slop oil / spill clean up material?

. . .

Has the sampled sand been re-stacked / segregated from daily inventory?

. . .

Have Truck/Loader/Vac truck Personnel been informed?

. . .

Is the sampled sand being hauled?

. . .

Has truck inspection been done?
(No sand loss)

. . .

Is there a Designated Truck Route ?

. . .

Has Notification of Affected Parties been Conducted?

. . .

Is the sand being applied to the proper depth and location for cells?

. . .

Is the sand being incorporated at a 1:3 ratio and at the proper location

. . .

Are truckloads being sampled?

. . .

Produced Sand Owner/Representative Name:_____________________ Date:______________

(print name)

Signature:________________________________

 

APPENDIX 5: Daily Road Information Check Sheet for Cells

APPENDIX 5

* Submit to MD or County and retain on file

DAILY ROAD INFORMATION CHECK SHEET FOR CELLS

ROAD INFORMATION

SOILS CONDITIONS REMARKS

DATE

COMMENTS / REMARKS

Survey Pin Numbers

Sand Delivery Composite per cell

Weather
(eg. 16°C, Cloudy)

Area of Cell              (m 2 )

Total Vol. per cell           (m 3)

Total cover
(depth)

Road Information

Sand Lens
Yes/No  

       .          

* If cell is closed due to rain, record actions taken. The cell maybe covered and continue when weather permits.                          

From

To

Sample / Comments

Before

During

After

. . .

New

Re-built

. . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .
. . . . . . . . . . . . . .

  • Additional items may include: as built plans submitted to MD/County

APPENDIX 6: Engineering & As-Built Plans

This section outlines the plan requirements industry must consider to incorporate or encapsulate produced sand into a statutory roads.

Required Engineering Plans

The mosaic plan/profile shall be prepared prior to construction and shall contain the following:

  • Profile of existing road surface or natural ground at centre line.
  • Profile of natural ground at each edge of the right-of-way.
  • Elevation of the design grade line and proposed ditch bottoms.
  • Elevation and location of proposed drainage structures.
  • Drainage plan for the area (0.8 km on either side of the road).
  • Typical cross-sections of proposed road.
  • Location and elevation of bench marks used for the survey and design.
  • Land locations on plan view.
  • Location and size of any water bodies including sloughs, ponds, dugouts, lakes, creeks, rivers, streams, and coulees into which surface drainage from the project could enter.
  • Existing and proposed right-of-way drafted on plan view.
  • Location of residences and any known water wells in the area.
  • Mass haul diagram.
  • Sections of road where produced sand will be placed indicating depth and width.
  • Bore hole test results.
  • Depth of water table encountered in test holes.

As-Built Plans

Upon completion of road construction, three copies of a signed and stamped engineering report documenting compliance with soil properties and the as-built plan/profile shall be prepared for the operator, County/Municipal District and the EUB. It should also contain the following information:

  • The location, width and depth of the produced sand incorporated or encapsulated into the road sub-grade.
  • The total amount of produced sand in tonnes incorporated or encapsulated into the road sub-grade.

Page Last Updated: August 1, 2002